This deviation is caused by the compressed air (nitrogen/oxygen mixture) used by FID detector, and has nothing to do with the quality of the sample itself. Acarbose: ①RSD meets the requirements; ② The samples were consistent with the historical test results, and no peaks were detected; ③ The baseline occurred between the end of the 9th needle and the beginning of the 10th needle in the sequence. Compared with the standard of the first 6 needles, the standard peak areas of the sample and the return needle are too large, so the detection is not affected, the data is valid, and there is no need to retest again; Epiavermectin, rosuvastatin calcium chiral side chain C2 (method 1), rosuvastatin calcium, rosuvastatin calcium chiral side chain C2 (method 2), and the results of emergency treatment measures were reported. Compressed air (nitrogen/oxygen mixture) used in this position in recent years is purchased from this supplier. Looking at the historical deviation in recent 2 years, there has been no deviation event caused by the confusion of two gases with different proportions, and the occurrence probability is relatively low, which does not bring risks to the early detection, and at the same time, the risks to the subsequent detection of the laboratory are controllable. Follow the column "root cause of deviation" on the left side.
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