Xiong et al. proposed that when CuAlO2 is synthesized by hydrothermal method, the formation of 2H and 3R is related to the addition of mineralizer NaOH. When NaOH is not added, a mixed phase of 2H and 3R is obtained. As the addition of NaOH increases, the 2H phase starts Reduce, when NaOH is added to 0.6 g, a pure 3R phase can be obtained
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